The effect of high energy ball milling under different conditions on the structure of Na +montmorillonite (NaMMT), and the organomontmorillonite (Cloisite 30B) was milling increased the structural disorder: peeling off of layers from the particles was observed, followed by the exfoliation of the particles, indicated by the disappearance of the (001) reflection.
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For stirred ballmilling intercalation, a ball mill (01HD, UNION PROCESS) was used in which samples were micronized in a Teflon pot using 2mm alumina balls. The device works through friction and impact via attrition rings and a cylinder inside a casing containing the sample. Grinding was extremely rapid. The sodiumexchanged montmorillonite was put into the milling tank with distilled water ...
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New organomontmorillonites were prepared by ball milling. • Their thermal stabilities were better than that of cationicorganomontmorillonite. • The first dspacings exceeded nm. • The preparation process was waterfree, simple, environmentally friendly. .
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· The OMMT was synthesized through the intercalation modification of sodium montmorillonite (NaMMT) with cationic cetyltrimethylammonium bromide (CTAB), nonionic nonylphenol polyoxyethylene ether (NPE) and the mixture of them via simple and convenient wet ballmilling method. Furthermore, the organomontmorillonite/alginate (OMMT/Alg) composite hydrogel beads with slow .
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